Subphthalocyanine-Based Porous Organic Polymers
4 and reduced on the rotovap to a yellow oil. Overnight the oil yields needle shaped crystals, which were swamped with MeOH and cooled in the fridge before filtering, washing with additional MeOH. Product isolated in 82% yield as white needly solids. 1H NMR (400 MHz CDCl 3) δ = 7.10 (s, 2H), 1.31 (m, 6H), 1.11 (d, 36H) 13C NMR (100 MHz CDCl
More details